AccScience Publishing / MSAM / Volume 1 / Issue 3 / DOI: 10.18063/msam.v1i3.16
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ORIGINAL RESEARCH ARTICLE

Optimizing of chemical admixtures for 3D printable cementitious materials by central composite design 

Mingyang Li1 Yiwei Weng2* Zhixin Liu1 Dong Zhang3 Teck Neng Wong1
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1 Singapore Centre for 3D Printing, Nanyang Technological University, Singapore
2 Department of Building and Real Estate, The Hong Kong Polytechnic University, Hong Kong, China
3 College of Civil Engineering, Fuzhou University, Fuzhou, China
Accepted: 4 September 2022 | Published: 21 September 2022
© 2022 by the Author(s). This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution 4.0 International License ( https://creativecommons.org/licenses/by/4.0/ )
Abstract

Printability of 3D printable cementitious materials is related to material rheological properties, and is affected and controlled by modern concrete chemical admixtures. In this work, the influence of several chemical admixtures including superplasticizer, retarder, and accelerator on the rheological characteristics of printable materials was investigated using central composite design (CCD). Twenty test points with varying dosages of chemical admixtures were performed to evaluate the primary effects of chemical admixtures and their combined interactive effects on the rheological properties. The results indicate that with the increase of retarder or superplasticizer dosage, all rheological parameters decrease while accelerator possesses an opposite impact. The rheological properties are negatively proportional to the combined interactive effect of retarder and accelerator. The combined interactive effect of retarder and superplasticizer positively affects dynamic yield stress, plastic viscosity, and thixotropy, while it negatively impacts static yield stress. The combined interactive effect of accelerator and retarder positively affects the yield stress, whereas it negatively influences the plastic viscosity and thixotropy. The results indicate that the CCD is an efficient method to find the desirable formulation within a given boundary.

Keywords
3D concrete printing
Central composites design
Rheological properties
Statistical models
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Materials Science in Additive Manufacturing, Electronic ISSN: 2810-9635 Published by AccScience Publishing